Bromomethylcyclopropane → 2-Bromo-1-(cyclopropylmethoxy)-4-ethylbenzene

反応式

[Br:1][C:2]1[CH:7]=[C:6]([CH2:8][CH3:9])[CH:5]=[CH:4][C:3]=1[OH:10].Br[CH2:12][CH:13]1[CH2:15][CH2:14]1>>[Br:1][C:2]1[CH:7]=[C:6]([CH2:8][CH3:9])[CH:5]=[CH:4][C:3]=1[O:10][CH2:12][CH:13]1[CH2:15][CH2:14]1

参加物

反応物 2

HCID 81503Bromomethylcyclopropane

HCID 166412522-Bromo-4-ethylphenol

生成物 1

HCID 670333542-Bromo-1-(cyclopropylmethoxy)-4-ethylbenzene

実験手順

Starting from 2-bromo-4-ethyl-phenol (example B.a5) and commercially available bromomethyl-cyclopropane the title compound is obtained as colorless oil after distillation at 10 mbar.

出典と根拠

ORDレコード: ord-8c76295549fc45b7959356b90ada2853
出典データセット: uspto-grants-2015_01
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08927557B2

反応ノート

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