Methyl 10-methylacridan-9-carboxylate → HCID 68467549、化合物
反応式
CN1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[CH:9]([C:16](Cl)=O)[C:8]2[CH:7]=[CH:6][CH:5]=CC1=2.[CH3:19][N:20]1[C:33]2[C:28](=[CH:29][CH:30]=[CH:31][CH:32]=2)[CH:27]([C:34]([O:36]C)=[O:35])[C:26]2[CH:25]=[CH:24][CH:23]=[CH:22][C:21]1=2>ClCCl.O1CCCC1>[CH3:19][N:20]1[C:33]2[C:28](=[CH:29][CH:30]=[CH:31][CH:32]=2)[CH:27]([C:34]([OH:36])=[O:35])[C:26]2[CH:25]=[CH:24][CH:23]=[CH:22][C:21]1=2.[CH:13]1[CH:12]=[CH:11][C:10]([C:9]2[CH:16]=[CH:5][CH:6]=[CH:7][CH:8]=2)=[CH:15][CH:14]=1参加物
5
実験手順
A solution of 0.24 parts of 10-methylacridan-9-carboxylic acid chloride (78) in 10 mL dichloromethane and 0.145 parts of 4-phenylphenol (76) in 5 mL of dichloromethane and 1 mL of tetrahydrofuran is treated as described in example I, to give 0.21 parts of 4,4′-biphenyl 10-methylacridan-9-carboxylate. This compound has the following structure.