反応式
[CH2:1]([NH2:5])[CH2:2][CH2:3][CH3:4].[CH3:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11].[C:12]([O:15]CC)(=[O:14])C>>[CH2:1]([NH:5][C:12](=[O:14])[O:15][C:8]1[CH:7]=[CH:6][CH:11]=[CH:10][CH:9]=1)[CH2:2][CH2:3][CH3:4]参加物
4
実験手順
n-Butylamine (4.9 ml, 50 mmol) was used for the same reaction as in Production Example 310-1, and purification was performed by silica gel column chromatography (hexane:ethyl acetate=4:1) to obtain the title compound (8.11 g, 41.97 mmol, 71.97%) as a colorless oil.
出典と根拠
- ORDレコード
- ord-1930a56b588b4759866ec40b97bfcb4d
- 出典データセット
- uspto-grants-2009_11
- 特許番号
- US07612092B2
関連ノート
読み込み中…