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6-Methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate → 7-Methoxy-3-(4-methoxy-2-nitrophenyl)-1,2-dihydronaphthalene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 6-Methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate | HCID 15330256 | — |
| 反応物 | Tributyl(4-methoxy-2-nitrophenyl)tin | HCID 23087474 | — |
| 生成物 | 7-Methoxy-3-(4-methoxy-2-nitrophenyl)-1,2-dihydronaphthalene | HCID 23087141 | 73.2% |
反応手順
Synthesized from 6-methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate (2.3 g) and tributyl(4-methoxy-2-nitrophenyl)tin (3.9 g) according to an analogous synthetic method to Preparation Example 77, the title compound (1.7 g) was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07612114B2 |
| 出典データセット | uspto-grants-2009_11 |
| ORD ID | ord-93695c5539284e51b554a25583905b0f |
| 出典メモ | uspto-grants-2009_11 |