Methylamine → N-methylpiperidine-2-carboxamide
反応式
C(O[N:9]1[CH2:14][CH2:13][CH2:12][CH2:11][CH:10]1[C:15]([OH:17])=O)C1C=CC=CC=1.[CH3:18][NH2:19]>O1CCCC1>[CH3:18][NH:19][C:15]([CH:10]1[CH2:11][CH2:12][CH2:13][CH2:14][NH:9]1)=[O:17]参加物
4
実験手順
The general procedure of Referential Example 131 was repeated through use of N-benzyloxypiperidine-2-carboxylic acid (2.0 g) and 1.0 M methylamine in tetrahydrofuran (4 mL), to thereby give the title compound as an oily product (970 mg, quantitative amount).
出典と根拠
- ORDレコード
- ord-e7d34bec75684832a71b0a225f0e3b6c
- 出典データセット
- uspto-grants-2009_11
- 特許番号
- US07622471B2
反応ノート
読み込み中…