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Benzaldehyde → N-Benzylidene(piperidin-4-yl)methanamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzaldehyde | HCID 240 | — |
| 反応物 | 4-(Aminomethyl)piperidine | HCID 23527 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | N-Benzylidene(piperidin-4-yl)methanamine | HCID 11820173 | — |
反応手順
Benzaldehyde (4.6 g; 0.044 mol) was added dropwise to a solution of 4-aminomethylpiperidine (5.0 g; 0.044 mol) in toluene (20 ml). The solution thus obtained was stirred for 3 h at room temperature. Then the solvent was removed by evaporation at reduced pressure and the residue was taken up twice with toluene to give the desired product that was used as such without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07662836B2 |
| 出典データセット | uspto-grants-2010_02 |
| ORD ID | ord-5924d5348ad944b5b28619e072e9943f |
| 出典メモ | uspto-grants-2010_02 |