Thionyl Chloride → 3-[[(4-Methoxy)phenylmethyl]thio]-2-methylthiopropionyl chloride

反応式

[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][S:10][CH2:11][CH:12]([CH3:16])[C:13](O)=[S:14])=[CH:5][CH:4]=1.S(Cl)([Cl:19])=O>>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][S:10][CH2:11][CH:12]([CH3:16])[C:13]([Cl:19])=[S:14])=[CH:5][CH:4]=1

参加物

反応物 2

HCID 24386Thionyl Chloride

HCID 178491718HCID 178491718、化合物

生成物 1

HCID 542258353-[[(4-Methoxy)phenylmethyl]thio]-2-methylthiopropionyl chloride

実験手順

3-[[(4-Methoxy)phenylmethyl]thio]-2-methylthiopropanoic acid prepared according to the procedure of Example 10 in U.S. Pat. No. 4,116,962 is treated with thionyl chloride to yield 3-[[(4-methoxy)phenylmethyl]-thio]-2-methylthiopropionyl chloride.

出典と根拠

ORDレコード: ord-6614dae488124144a9422e514c270a19
出典データセット: uspto-grants-1982_02
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04316905

反応ノート

読み込み中…