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Benzene → 2-(4-Methoxyphenyl)-2-methyl-5-benzyloxy-6,7-dichloro-1-indanone

HRID 1447673
ノート
印刷プレビュー

反応式

HRID 1447673 の反応式
C[C:2](C)([O-:4])C.[K+].[CH3:7][CH:8]1[CH2:16][C:15]2[C:10](=[C:11]([Cl:26])[C:12]([Cl:25])=[C:13]([O:17][CH2:18][C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[CH:14]=2)[C:9]1=[O:27].[CH:28]1[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=1.O>C(O)(C)(C)C>[CH3:2][O:4][C:28]1[CH:33]=[CH:32][C:31]([C:8]2([CH3:7])[CH2:16][C:15]3[C:10](=[C:11]([Cl:26])[C:12]([Cl:25])=[C:13]([O:17][CH2:18][C:19]4[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=4)[CH:14]=3)[C:9]2=[O:27])=[CH:30][CH:29]=1
参加物反応条件実験手順後処理出典と根拠反応ノート

参加物

6

反応物 4

HCID 241BenzeneHCID 962WaterHCID 124236142-Methyl-5-benzyloxy-6,7-dichloro-1-indanoneHCID 23665647Potassium tert-butoxide

生成物 1

HCID 124236152-(4-Methoxyphenyl)-2-methyl-5-benzyloxy-6,7-dichloro-1-indanone

試薬・触媒・溶媒 1

HCID 6386tert-Butanol溶媒2 回

反応条件

温度
25 °C

実験手順

Potassium tert-butoxide (8.42 g., 0.075 mole) dissolved in tert-butanol (450 ml.) is added to a refluxing solution of 2-methyl-5-benzyloxy-6,7-dichloro-1-indanone (16.1 g., 0.05 mole) in tert-butanol (150 ml.)-benzene (600 ml.), refluxing is continued for 2.5 hrs., then 4,4'-dimethoxydiphenyliodonium chloride (37.66 g., 0.10 mole) is added and refluxing is continued for 3 hrs. The reaction mixture is cooled to 25° C., 500 ml. water added, and the mixture concentrated in vacuo to give a brown oil which on ether extraction, drying over anhydrous magnesium sulfate, removal of the ether and chromatographing of the residue on silica gel with chloroform gives 3.44 g. of 2-(4-methoxyphenyl)-2-methyl-5-benzyloxy-6,7-dichloro-1-indanone which melts at 115°-119° C. and is used without further purification.

後処理

  1. temperaturerefluxing
  2. temperaturerefluxing
  3. waitis continued for 3 hrs
  4. concentrationthe mixture concentrated in vacuo
  5. customto give a brown oil which
  6. extractionon ether extraction
  7. dry with materialdrying over anhydrous magnesium sulfate, removal of the ether and chromatographing of the residue on silica gel with chloroform
  8. customgives 3.44 g
  9. customof 2-(4-methoxyphenyl)-2-methyl-5-benzyloxy-6,7-dichloro-1-indanone which melts at 115°-119° C. and is used without further purification

出典と根拠

ORDレコード
ord-5921716aea884320a57bc9c02d04f217
出典データセット
uspto-grants-1979_12
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US04177285

反応ノート

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