2-Butanethiol → Di-sec-butyl disulfide
反応式
[CH3:1][CH:2]([SH:5])[CH2:3][CH3:4]>C(#N)C>[CH3:1][CH:2]([S:5][S:5][CH:2]([CH3:1])[CH2:3][CH3:4])[CH2:3][CH3:4]参加物
3
試薬・触媒・溶媒 1
実験手順
A solution of 150 μg of LL-E33288γ1 -I in 1 ml of acetonitrile was treated with 50 μl of a 1 μmole/ml solution of 1-methyl-1-propyl mercaptan. After 2 hours, the reaction was complete, giving the desired 1-methyl-1-propyl disulfide of LL-E33288γ1 -I.
出典と根拠
- ORDレコード
- ord-c15de9c81da446228f35a93da269be60
- 出典データセット
- uspto-grants-1997_02
- 特許番号
- US05606040
反応ノート
読み込み中…