Sodium Hydroxide → 5-Ethoxymethyl-6-methyl-pyridin-2-ylamine
反応式
[CH2:1]([O:3][CH2:4][C:5]1[CH:6]=[CH:7][C:8]([NH:12]C(=O)C(C)(C)C)=[N:9][C:10]=1[CH3:11])[CH3:2].[OH-].[Na+]>>[CH2:1]([O:3][CH2:4][C:5]1[CH:6]=[CH:7][C:8]([NH2:12])=[N:9][C:10]=1[CH3:11])[CH3:2]参加物
3
実験手順
This material was prepared in analogy to example 86 step B] from N-(5-ethoxymethyl-6-methyl-pyridin-2-yl)-2,2-dimethyl-propionamide (0.32 g) and 3M aqueous NaOH (2.62 mL) as a yellow oil (0.28 g) that was used directly in the next step.
出典と根拠
- ORDレコード
- ord-260856e1cf7a460982668da25a610f54
- 出典データセット
- uspto-grants-2009_01
- 特許番号
- US07482341B2
反応ノート
読み込み中…