Water → 2-Methoxy-5-tetrazol-1-yl-benzaldehyde
反応式
[OH:1][C:2]1[CH:9]=[CH:8][C:7]([N:10]2[CH:14]=[N:13][N:12]=[N:11]2)=[CH:6][C:3]=1[CH:4]=[O:5].[C:15](=O)([O-])[O-].[K+].[K+].IC.O>CN(C)C=O>[CH3:15][O:1][C:2]1[CH:9]=[CH:8][C:7]([N:10]2[CH:14]=[N:13][N:12]=[N:11]2)=[CH:6][C:3]=1[CH:4]=[O:5]参加物
6
実験手順
To a solution of 2-hydroxy-5-tetrazol-1-yl-benzaldehyde (2.63 mmol) in dimethylformamide (5 ml) was added potassium carbonate (3.95 mmol) and iodomethane (3.95 mmol) and the mixture was stirred under nitrogen atmosphere for 2 h. The mixture was poured into water (100 ml) and the white solid formed filtered to afford the title compound in a 67% yield.
後処理
- customthe white solid formed
- filtrationfiltered
出典と根拠
- ORDレコード
- ord-b5e9d024b04a4956af7e7f333ec2180e
- 出典データセット
- uspto-grants-1998_12
- 特許番号
- US05843966
反応ノート
読み込み中…