Methylamine → HCID 59896620、化合物

HRID 1457901ノート

反応式

HRID 1457901 の反応式
[Cl:1][C:2]1[N:7]=[CH:6][C:5]([CH2:8][NH:9][C:10](SC)=[CH:11][N+:12]([O-:14])=[O:13])=[CH:4][CH:3]=1.O.[NH2:18][NH2:19].CSC(NCC1C=NC=CC=1)=C[N+]([O-])=O.CN>>[Cl:1][C:2]1[N:7]=[CH:6][C:5]([CH2:8][NH:9][C:10]([NH:18][NH2:19])=[CH:11][N+:12]([O-:14])=[O:13])=[CH:4][CH:3]=1

参加物

5

反応物 4

HCID 6329MethylamineHCID 24654Hydrazine hydrate (1:1)HCID 70155832HCID 70155832、化合物HCID 855929321-(6-Chloro-3-pyridylmethyl)amino-1-methylthio-2-nitroethylene

生成物 1

HCID 59896620HCID 59896620、化合物

実験手順

The reaction procedure of Example 3 was repeated except that 1-(6-chloro-3-pyridylmethyl)amino-1-methylthio-2-nitroethylene and hydrazine hydrate were used in lieu of 1-methylthio-1-(3-pyridylmethyl)amino-2-nitroethylene and aqueous methylamine solution, respectively. The procedure gave the title compound as pale yellow crystals.

後処理

  1. customThe reaction procedure of Example 3

出典と根拠

ORDレコード
ord-7719f56430f14d6093c33d6c43fd1696
出典データセット
uspto-grants-1998_12
特許番号
US05849768

反応ノート

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