反応式
[CH3:1][NH:2][CH3:3].[C:4](=[S:6])=[S:5]>>[CH3:1][N:2]([CH3:4])[C:3](=[S:6])[S:5][S:5][C:4](=[S:6])[N:2]([CH3:3])[CH3:1]参加物
3
実験手順
The work was carried out as in Example 3, but now the rate of addition of carbon disulfide corresponded to the rate at which dimethylamine was released during the reaction. No further carbon disulfide was added after 46 minutes and the reaction had ended after 49 minutes. This method yielded a total of 35.85 g of tetramethyl thiuram disulfide, corresponding to 99.6% of theoretical.
後処理
- customwas released during the reaction
出典と根拠
- ORDレコード
- ord-0574f614f5e04347bb14d3948a907c4e
- 出典データセット
- uspto-grants-1984_07
- 特許番号
- US04459424
関連ノート
読み込み中…