反応式
FC(O[C:5]1[C:10]([CH3:11])=[CH:9][CH:8]=[CH:7][C:6]=1[CH3:12])=O.[FH:13]>>[CH3:12][C:6]1[CH:7]=[CH:8][CH:9]=[C:10]([CH3:11])[C:5]=1[F:13]参加物
3
反応条件
- 温度
- 140 °C
実験手順
200 ml of anhydrous hydrogen fluoride were placed at 0° C. in a stainless steel laboratory autoclave and 100 g of 2,6-dimethylphenyl fluoroformate were added dropwise. The autoclave was sealed and heated at a maximum temperature of 140° C. for 1.5 hours. The reaction mixture was worked up as described in Example 9. 2,6-Dimethylfluorobenzene was obtained in a yield of 75%.
後処理
- additionwere added dropwise
- customThe autoclave was sealed
出典と根拠
- ORDレコード
- ord-0378ee7987964b1e8d46c22a9b389338
- 出典データセット
- uspto-grants-1994_04
- 特許番号
- US05306849
関連ノート
読み込み中…