Sulfuric Acid → 2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide sulfate

HRID 1476706

反応式

HRID 1476706 の反応式
[NH2:1][C:2]1[CH:18]=[CH:17][CH:16]=[C:15]([S:19][C:20]2[CH:25]=[CH:24][C:23]([N+:26]([O-:28])=[O:27])=[CH:22][CH:21]=2)[C:3]=1[C:4]([NH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[O:13][CH3:14])=[O:5].[OH:29][S:30]([OH:33])(=[O:32])=[O:31]>CC(=O)OCC>[S:30]([OH:33])([OH:32])(=[O:31])=[O:29].[NH2:1][C:2]1[CH:18]=[CH:17][CH:16]=[C:15]([S:19][C:20]2[CH:21]=[CH:22][C:23]([N+:26]([O-:28])=[O:27])=[CH:24][CH:25]=2)[C:3]=1[C:4]([NH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[O:13][CH3:14])=[O:5]

参加物

4

反応物 2

HCID 1118Sulfuric AcidHCID 718115872-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide

生成物 1

HCID 1183870042-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide sulfate収率 72%

試薬・触媒・溶媒 1

HCID 8857Ethyl Acetate溶媒

実験手順

2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide dissolved in EA, stirred at room temperature, while dropped H2SO4 into mixture till occurred to white solid. The reaction mixture was filtered to get White solid; 72% yield;

後処理

  1. filtrationThe reaction mixture was filtered
  2. customto get White solid

出典と根拠

ORDレコード
ord-46c5fcb07c94481a8e8f0d3a8d9e85a9
出典データセット
uspto-grants-2016_08
特許番号
US09402819B2

関連ノート

読み込み中…