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2-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline → HCID 89996038、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline | HCID 17750207 | — |
| 反応物 | (4-bromo-1-methyl-1H-pyrazol-5-yl)methanol | HCID 57415773 | — |
| 生成物 | HCID 89996038 | HCID 89996038 | — |
反応手順
The title compound was prepared according to the method described for Preparation 158 using (4-bromo-1-methyl-1H-pyrazol-5-yl)methanol (Preparation 222) and 2-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline. The residue was purified using Biotage silica gel column chromatography eluting with EtOAc followed by elution through an SCX-2 cartridge.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09409907B2 |
| 出典データセット | uspto-grants-2016_08 |
| ORD ID | ord-bcb834331b3f43909113504e5aa25ee0 |
| 出典メモ | uspto-grants-2016_08 |