Acrylic Acid → Trichlorogermylpropionic acid

反応式

[Cl:1][GeH:2]([Cl:4])[Cl:3].[C:5]([OH:9])(=[O:8])[CH:6]=[CH2:7]>>[Cl:1][Ge:2]([CH:6]([CH3:7])[C:5]([OH:9])=[O:8])([Cl:4])[Cl:3]

参加物

反応物 2

HCID 6581Acrylic Acid

HCID 70900CID 70900

生成物 1

HCID 13587901Trichlorogermylpropionic acid

実験手順

Trichlorogermane (Cl3GeH) was added to acrylic acid (CH2CHCOOH) to obtain trichlorogermylpropionic acid (Cl3GeCH2CH2 COOH). It was hydrolyzed to synthesize an organogermanium compound (1). In the same manner were synthesized organogermanium compounds (2) to (51).

出典と根拠

ORDレコード: ord-475a9231fe514e16b33ca026b4a3a09a
出典データセット: uspto-grants-1997_10
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05679787

反応ノート

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