反応式
CCSc1ccccc1>C1=CCCC=CCC1.C1=CCCC=CCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1ccc(C)cc1.Cc1ccnc(-c2cc(C)ccn2)c1.[Ir].[Ir]>CCSc1cccc(B2OC(C)(C)C(C)(C)O2)c1.CCSc1ccccc1B1OC(C)(C)C(C)(C)O1参加物
7
反応物 1
生成物 2
試薬・触媒・溶媒 4
反応条件
- 温度
- 55 °C
実験手順
dtbpy: The mixture of product (110 mg, 83% yield, ortho/meta + para = 0.29); meta- and para- isomers (5b+5bʹ) were obtained by further purification of the crude mixture by GPC (77 mg, 58% yield), colorless oil;
出典と根拠
- ORDレコード
- ord-3cf848853d454210a4ad7b64186a1c6e
- 出典データセット
- Borylation dataset from Roche
関連ノート
読み込み中…