Thionyl Chloride → 2-Amino-3-nitrobenzoyl chloride
反応式
[NH2:1][C:2]1[C:10]([N+:11]([O-:13])=[O:12])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4](O)=[O:5].S(Cl)([Cl:16])=O>>[NH2:1][C:2]1[C:10]([N+:11]([O-:13])=[O:12])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([Cl:16])=[O:5]参加物
3
実験手順
A mixture of 9.90 parts of 2-amino-3-nitrobenzoic acid and 32.4 parts of thionyl chloride was stirred for 15 min at reflux temperature under argon. The excess of thionyl chloride was evaporated, yielding 10.8 parts (100%) of 2-amino-3-nitrobenzoyl chloride (interm. 39).
後処理
- temperatureat reflux temperature under argon
- customThe excess of thionyl chloride was evaporated
出典と根拠
- ORDレコード
- ord-80550d19bae04b9e93fce46bcb97b910
- 出典データセット
- uspto-grants-1994_12
- 特許番号
- US05371079
反応ノート
読み込み中…