Methyl iodide → HCID 178503978、化合物

HRID 1492211ノート

反応式

HRID 1492211 の反応式
[O:1]1[CH2:6][CH2:5][N:4]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=2[NH:13][C:14]([NH2:16])=[S:15])[CH2:3][CH2:2]1.[CH3:17][I:18]>CO>[IH:18].[CH3:17][S:15][C:14](=[NH:16])[NH:13][C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=1[N:4]1[CH2:5][CH2:6][O:1][CH2:2][CH2:3]1

参加物

4

反応物 2

HCID 6328Methyl iodideHCID 27411931-(2-Morpholinophenyl)thiourea

生成物 1

HCID 178503978HCID 178503978、化合物

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

A solution of 1-(2-morpholinophenyl)thiourea (7.2 g) in dry methanol (30 ml) was heated at reflux with methyliodide (4.2 g) for 2 hours. The solvent was removed under reduced pressure and dry ether (15 ml) was added and on scratching gave 2-methyl-1-(2-morpholinophenyl)-2-thiopseudourea hydroiodide (m.p. 151°-152° C.).

後処理

  1. customThe solvent was removed under reduced pressure and dry ether (15 ml)
  2. additionwas added

出典と根拠

ORDレコード
ord-cad3fee50b7346f5b53ce7976e22d40d
出典データセット
uspto-grants-1994_12
特許番号
US05373008

反応ノート

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