Dodecylammonium chloride → HCID 178443247、化合物

HRID 1492982ノート

反応式

HRID 1492982 の反応式
[C:1]([NH:3][C:4]([NH:6][CH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[NH:5])#[N:2].[ClH:14].[CH2:15]([NH2:27])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]>C1(C)C=C(C)C=C(C)C=1>[ClH:14].[CH2:7]([NH:6][C:4]([NH:3][C:1]([NH:27][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26])=[NH:2])=[NH:5])[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1

参加物

4

反応物 2

HCID 458426Dodecylammonium chlorideHCID 178512368HCID 178512368、化合物

生成物 1

HCID 178443247HCID 178443247、化合物収率 52.3%

試薬・触媒・溶媒 1

HCID 7947Mesitylene溶媒

実験手順

To 20 g of N1 -cyano-N3 -benzyl-guanidine and 25.4 g of dodecylamine hydrochloride, 200 ml of mesitylene was added, which was heated and refluxed for 2 hours. After reaction, by the same operation as in Example 1, 23.7 g of the captioned compound was obtained.

後処理

  1. temperaturewhich was heated
  2. temperaturerefluxed for 2 hours
  3. customAfter reaction

出典と根拠

ORDレコード
ord-43889fa667fd4712ae723990d24f7a92
出典データセット
uspto-grants-1994_12
特許番号
US05376686

反応ノート

読み込み中…