Methacrylic Acid → Copper(2+) bis(2-methylprop-2-enoate)

HRID 1493114ノート

反応式

HRID 1493114 の反応式
[O-]CC.[Cu+2:4].[O-]CC.[C:8]([OH:13])(=[O:12])[C:9]([CH3:11])=[CH2:10]>O1CCCC1>[C:8]([O-:13])(=[O:12])[C:9]([CH3:11])=[CH2:10].[Cu+2:4].[C:8]([O-:13])(=[O:12])[C:9]([CH3:11])=[CH2:10]

参加物

4

反応物 2

HCID 4093Methacrylic AcidHCID 14419876Ethanol, copper(2 ) salt

生成物 1

HCID 6452881Copper(2+) bis(2-methylprop-2-enoate)

試薬・触媒・溶媒 1

HCID 8028Tetrahydrofuran溶媒

実験手順

1.50 Grams (0.009 mol) of copper (II) ethoxide was introduced into a 50 ml. round bottom flask having a magnetic spinning bar, in an argon atmosphere in a dry box. A solution of 1.84 g (0.02 mol) of methacrylic acid, prepared in 20 ml of anhydrous tetrahydrofuran was then added to it. The contents of the flask were agitated overnight (20 hr) by means of a magnetic stirrer at ambient temperature under argon. All volatile matter was then removed in vacuo (about 0.1 mm Hg) for 12 hours. The resulting solid was analyzed for its metal content.

後処理

  1. customround bottom flask having
  2. additionwas then added to it
  3. customAll volatile matter was then removed in vacuo (about 0.1 mm Hg) for 12 hours

出典と根拠

ORDレコード
ord-7947042a76134bc88e2f125442b117f5
出典データセット
uspto-grants-1991_06
特許番号
US05021398

反応ノート

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