2-Phenoxy-1-propanol → 2-Phenoxypropanol sulfamate

HRID 1493987

反応式

HRID 1493987 の反応式
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[O:6]([CH:13]([CH3:16])[CH2:14][OH:15])[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1>>[O:6]([CH:13]([CH3:16])[CH2:14][O:15][S:1](=[O:4])(=[O:3])[NH2:2])[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1

参加物

3

反応物 2

HCID 201292-Phenoxy-1-propanolHCID 24499Chlorosulfamic acid

生成物 1

HCID 191086852-Phenoxypropanol sulfamate

実験手順

The title compound was prepared by procedures of Example 16 from sulfamoyl chloride and 2-phenoxypropanol. The oil obtained was further purified by chromatography (silica gel, eluted with methylene chloride) and recrystallization to give the title compound as a colorless, viscous oil in 35% yield.

後処理

  1. customThe oil obtained
  2. customwas further purified by chromatography (silica gel, eluted with methylene chloride) and recrystallization

出典と根拠

ORDレコード
ord-49b84d7750004e6d8ebe2201632d38d3
出典データセット
uspto-grants-1991_06
特許番号
US05025031

関連ノート

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