化工社化工社 化学情報印刷レポート · 研究参考用
2-Phenoxy-1-propanol → 2-Phenoxypropanol sulfamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Phenoxy-1-propanol | HCID 20129 | — |
| 反応物 | Chlorosulfamic acid | HCID 24499 | — |
| 生成物 | 2-Phenoxypropanol sulfamate | HCID 19108685 | — |
反応手順
The title compound was prepared by procedures of Example 16 from sulfamoyl chloride and 2-phenoxypropanol. The oil obtained was further purified by chromatography (silica gel, eluted with methylene chloride) and recrystallization to give the title compound as a colorless, viscous oil in 35% yield.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05025031 |
| 出典データセット | uspto-grants-1991_06 |
| ORD ID | ord-49b84d7750004e6d8ebe2201632d38d3 |
| 出典メモ | uspto-grants-1991_06 |