Lauryldimethylamine → Benzenemethanaminium, N-dodecyl-4-ethenyl-N,N-dimethyl-, chloride (1:1)
反応式
[CH:1]([C:3]1[CH:10]=[CH:9][C:6]([CH2:7][Cl:8])=[CH:5][CH:4]=1)=[CH2:2].[CH3:11][N:12]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])[CH3:13]>>[Cl-:8].[CH3:11][N+:12]([CH3:13])([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])[CH2:7][C:6]1[CH:9]=[CH:10][C:3]([CH:1]=[CH2:2])=[CH:4][CH:5]=1参加物
3
実験手順
Into a 200 ml flask were added 29.8 g of 4-vinylbenzyl chloride and 50 g of N,N-dimethyldodecylamine. The reaction mixture was stirred at room temperature for 24 h. The solid precipitate from the reaction was filtered, washed with diethyl ether, and dried under vacuum at room temperature.
後処理
- filtrationThe solid precipitate from the reaction was filtered
- washwashed with diethyl ether
- customdried under vacuum at room temperature
出典と根拠
- ORDレコード