Sodium Hydroxide → 9-Decenoic acid
反応式
C[O:2][C:3](=[O:13])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH:11]=[CH2:12].[OH-].[Na+]>>[C:3]([OH:13])(=[O:2])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH:11]=[CH2:12]参加物
3
実験手順
9-decenoic acid methyl ester prepared according to the method set forth in Example 12 is isolated then hydrolyzed under basic conditions (reflux with an excess of dilute aqueous NaOH), followed by removal of methanol. The resulting aqueous solution is then treated with an excess of dilute HCl, and the solution is distilled to provide 9-decenoic acid. Oligomers are then prepared according to the methods set forth in Examples 1 and 2, wherein the oleic acid is replaced with 9-decenoic acid.
後処理
- customis isolated
- customfollowed by removal of methanol
- additionThe resulting aqueous solution is then treated with an excess of dilute HCl
- distillationthe solution is distilled
出典と根拠
- ORDレコード
- ord-197a860dcbb94862b6f7d4a9885b5a9a
- 出典データセット
- uspto-grants-2015_12
- 特許番号
- US09199911B2
反応ノート
読み込み中…