Neopentyl glycol → tert-Butyl 2-(3-hydroxy-2,2-dimethylpropoxymethyl)-6-methylbenzoate
反応式
Br[CH2:2][C:3]1[CH:15]=[CH:14][CH:13]=[C:12]([CH3:16])[C:4]=1[C:5]([O:7][C:8]([CH3:11])([CH3:10])[CH3:9])=[O:6].[CH3:17][C:18]([CH3:23])([CH2:21][OH:22])[CH2:19][OH:20].OCCCOCC1C=CC=C(C)C=1C(OC(C)(C)C)=O>>[OH:20][CH2:19][C:18]([CH3:23])([CH3:17])[CH2:21][O:22][CH2:2][C:3]1[CH:15]=[CH:14][CH:13]=[C:12]([CH3:16])[C:4]=1[C:5]([O:7][C:8]([CH3:11])([CH3:10])[CH3:9])=[O:6]参加物
4
実験手順
tert-Butyl 2-(3-hydroxy-2,2-dimethylpropoxymethyl)-6-methylbenzoate is prepared from tert-butyl 2-bromomethyl-6-methylbenzoate and 2,2-dimethylpropane-1,3-diol in analogy to the synthesis of tert-butyl 2-(3-hydroxypropoxymethyl)-6-methylbenzoate.
出典と根拠
- ORDレコード
- ord-567678157c9e4668a470f15f1995b5e5
- 出典データセット
- uspto-grants-2010_06
- 特許番号
- US07732471B2
反応ノート
読み込み中…