5-Bromosalicylaldehyde → HCID 178449915、化合物

HRID 1531248

反応式

HRID 1531248 の反応式
[Br:1][C:2]1[CH:3]=[CH:4][C:5]([OH:10])=[C:6]([CH:9]=1)[CH:7]=O.[C:11]([NH:15][OH:16])([CH3:14])([CH3:13])[CH3:12]>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([OH:10])=[C:6]([CH:7]=[N+:15]([C:11]([CH3:14])([CH3:13])[CH3:12])[O-:16])[CH:9]=1

参加物

3

反応物 2

HCID 728635-BromosalicylaldehydeHCID 98586N-tert-butylhydroxylamine

生成物 1

HCID 178449915HCID 178449915、化合物

実験手順

The title compound was prepared according to the procedure described in Example 1 using 5-bromo-2-hydroxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 68.7% yield as a yellow crystalline solid, m.p. 118.7° C. (Rf=0.65 on a silica gel plate using 1:1 EtOAc/hexanes as an eluant).

後処理

  1. customThe title compound was prepared

出典と根拠

ORDレコード
ord-de7a2748ebe648fd8b933d3c61c58394
出典データセット
uspto-grants-2001_03
特許番号
US06197826B1

関連ノート

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