Formaldehyde → Cyclohexylhydroxymethylphosphinic acid, n-butyl ester

HRID 1535

反応式

HRID 1535 の反応式
[CH:1]1([PH:7](=[O:13])[O:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH2:14]=[O:15]>>[CH:1]1([P:7]([CH2:14][OH:15])(=[O:13])[O:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

参加物

3

反応物 2

HCID 712FormaldehydeHCID 178418445HCID 178418445、化合物

生成物 1

HCID 53866528Cyclohexylhydroxymethylphosphinic acid, n-butyl ester

実験手順

The title compound was prepared from cyclohexylphosphinic acid, n-butyl ester and paraformaldehyde according to the method described in Procedure 31. Purification by chromatography, eluting with dichloromethane containing 5% methanol, gave an oil.

後処理

  1. customPurification by chromatography
  2. washeluting with dichloromethane containing 5% methanol
  3. customgave an oil

出典と根拠

ORDレコード
ord-8779dd64d7dd4ab6a8cba54d39669391
出典データセット
uspto-grants-1998_03
特許番号
US05726165

関連ノート

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