5-[3-(N-Benzyl-N-ethylamino)-propyl]-5H-dibenzo[a,d]cycloheptene → 5-(3-ethylaminopropyl)-5H-dibenzo[a,d]cycloheptene
反応式
[CH2:1]([N:8]([CH2:11][CH2:12][CH2:13][CH:14]1[C:20]2[CH:21]=[CH:22][CH:23]=[CH:24][C:19]=2[CH:18]=[CH:17][C:16]2[CH:25]=[CH:26][CH:27]=[CH:28][C:15]1=2)CC)[C:2]1C=CC=CC=1>[Pd]>[CH2:1]([NH:8][CH2:11][CH2:12][CH2:13][CH:14]1[C:15]2[CH:28]=[CH:27][CH:26]=[CH:25][C:16]=2[CH:17]=[CH:18][C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][C:20]1=2)[CH3:2]参加物
3
実験手順
5-[3-(N-Benzyl-N-ethylamino)-propyl]-5H-dibenzo[a,d]cycloheptene is dissolved in absolute alcohol and hydrogenated over palladium on alumina catalyst at 40°-60°C. The catalyst is separated and the product isolated by evaporating the solvent.
後処理
- customThe catalyst is separated
- customthe product isolated
- customby evaporating the solvent
出典と根拠
- ORDレコード
- ord-d987f8c8360344feb265138d50e95f68
- 出典データセット
- uspto-grants-1976_09
- 特許番号
- US03981917
反応ノート
読み込み中…