Allyl iodide → Allyl Hexadecyl Dimethyl Ammonium Iodide

HRID 1578422

反応式

HRID 1578422 の反応式
[CH2:1]([I:4])[CH:2]=[CH2:3].[CH3:5][N:6]([CH3:23])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]>C(OCC)(=O)C>[I-:4].[CH2:1]([N+:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])([CH3:5])[CH3:23])[CH:2]=[CH2:3]

参加物

4

反応物 2

HCID 11166Allyl iodideHCID 16221Dimethylhexadecylamine

生成物 1

HCID 21391586Allyl Hexadecyl Dimethyl Ammonium Iodide

試薬・触媒・溶媒 1

HCID 8857Ethyl Acetate溶媒

実験手順

16.8 grams of allyl iodide were dissolved in 44.6 grams of ethyl acetate and 27.8 grams of dimethyl hexadecyl amine were added slowly with stirring at room temperature. Within 15 minutes after the addition of the amine was complete, the viscosity of the solution increased and crystallization occurred. After 24 hours the crystals were filtered, washed with ethyl acetate, and dried. The colorless crystalline product contained 88% of the theoretical amount of iodide ion.

後処理

  1. temperaturethe viscosity of the solution increased
  2. customcrystallization
  3. filtrationAfter 24 hours the crystals were filtered
  4. washwashed with ethyl acetate
  5. customdried

出典と根拠

ORDレコード
ord-aa6c198508d64d179de3385d0f4d93c1
出典データセット
uspto-grants-1976_02
特許番号
US03936492

関連ノート

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