Acetohydrazide → HCID 178475140、化合物
反応式
[CH3:1][N:2]1[C:6]([N+:7]([O-:9])=[O:8])=[CH:5][N:4]=[C:3]1[C:10](=[NH:14])OCC.[C:15]([NH:18][NH2:19])(=[O:17])[CH3:16]>CO>[CH3:1][N:2]1[C:6]([N+:7]([O-:9])=[O:8])=[CH:5][N:4]=[C:3]1[C:10]([NH:19][NH:18][C:15](=[O:17])[CH3:16])=[NH:14]参加物
4
実験手順
In 200 ml. of methanol, 12 g. (0.06 mole) of ethyl 1-methyl-5-nitro-2-imidazolecarboximidate and 4.9 g. (0.066 mole) of acetyl hydrazine are refluxed for 30 hours. The yellow compound is collected, washed with cold methanol and dried to give 12.97 g. of the title compound, melting point 294°C.
後処理
- customThe yellow compound is collected
- washwashed with cold methanol
- customdried
- customto give 12.97 g
出典と根拠
- ORDレコード
- ord-6646db82708743fe97c41ba1da41885f
- 出典データセット
- uspto-grants-1976_02
- 特許番号
- US03940411
反応ノート
読み込み中…