HCID 68139236、化合物 → HCID 68139039、化合物
反応式
[CH3:1][O:2][C:3]1[CH:10]=[C:9]([C:11]([CH3:22])=[C:12]([CH3:21])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])[CH:8]=[C:5]([O:6][CH3:7])[CH:4]=1>C(O)C.[Pd]>[CH3:7][O:6][C:5]1[CH:8]=[C:9]([CH:11]([CH3:22])[CH:12]([CH3:21])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])[CH:10]=[C:3]([O:2][CH3:1])[CH:4]=1参加物
4
実験手順
Dehydration by distillation from a few drops of 20% aqueous sulfuric acid gives a mixture of 5-(1,2-dimethyldec-1-enyl)resorcinol dimethyl ether and 5-(1-methylenyl-2-methyldecyl)resorcinol dimethyl ether which is hydrogenated over 10% palladium-on-carbon in absolute ethanol at 50 p.s.i. and 25° to give 5-(1,2-dimethyldecyl)-resorcinol dimethyl ether.
後処理
- distillationDehydration by distillation from a few drops of 20% aqueous sulfuric acid
- customgives