p-Anisoyl chloride → HCID 21561634、化合物
反応式
Cl.[OH:2][CH2:3][C:4]1[CH:5]=[C:6]([OH:11])[C:7]([CH3:10])=[N:8][CH:9]=1.[C:12](Cl)(=[O:21])[C:13]1[CH:18]=[CH:17][C:16]([O:19][CH3:20])=[CH:15][CH:14]=1>N1C=CC=CC=1>[OH:2][CH2:3][C:4]1[CH:5]=[C:6]([O:11][C:12](=[O:21])[C:13]2[CH:18]=[CH:17][C:16]([O:19][CH3:20])=[CH:15][CH:14]=2)[C:7]([CH3:10])=[N:8][CH:9]=1参加物
4
実験手順
To a solution of 0.9 g. of 5-hydroxymethyl-2-methyl-3-pyridinol hydrochloride in 5 ml. of anhydrous pyridine was added 0.86 g. of p-anisoyl chloride dropwise under cooling. After standing overnight the resulting mixture was poured into ice water and extracted with chloroform.
後処理
- extractionextracted with chloroform
出典と根拠
- ORDレコード
- ord-15bcc5cc87684b72b11f6ed65c6b3fbf
- 出典データセット
- uspto-grants-1976_01
- 特許番号
- US03935311
反応ノート
読み込み中…