Hydrogen Bromide → HCID 86740489、化合物
反応式
[BrH:1].[CH2:2]([O:4][C:5](=[O:30])[C@H:6]([CH2:22][C:23]1[CH:28]=[CH:27][C:26]([OH:29])=[CH:25][CH:24]=1)[NH:7][C:8](=[O:21])[CH2:9][NH:10]C(OCC1C=CC=CC=1)=O)[CH3:3].C(OCC)C>C(O)(=O)C>[CH2:2]([O:4][C:5](=[O:30])[C@H:6]([CH2:22][C:23]1[CH:28]=[CH:27][C:26]([OH:29])=[CH:25][CH:24]=1)[NH:7][C:8](=[O:21])[CH2:9][NH2:10])[CH3:3].[BrH:1]参加物
5
実験手順
250 ml of 25% HBr in glacial acetic acid was added to carbobenzoxyglycyl-L-tyrosine ethyl ester obtained above, and after the mixture was stirred for 30 minutes at room temperature, 5 l of absolute ethyl ether was added to the mixture to produce a precipitate. The precipitate was washed with ethyl ether to obtain glycyl-L-tyrosine ethyl ester·HBr.
後処理
- customobtained above, and after the mixture
- customto produce a precipitate
- washThe precipitate was washed with ethyl ether
出典と根拠
- ORDレコード
- ord-1ce7a0560cc043c6b8367090b75dc9aa
- 出典データセット
- uspto-grants-1985_11
- 特許番号
- US04551272
反応ノート
読み込み中…