化工社化工社 化学情報印刷レポート · 研究参考用
Boric Acid → Calcium;2,3-dihydroxy-3-[2-hydroxy-5-(hydroxymethyl)-1,3,2-dioxaborolan-4-yl]propanoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Boric Acid | HCID 7628 | — |
| 反応物 | Gluconic Acid | HCID 10690 | — |
| 反応物 | Calciumoxide | HCID 6850728 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Calcium;2,3-dihydroxy-3-[2-hydroxy-5-(hydroxymethyl)-1,3,2-dioxaborolan-4-yl]propanoate | HCID 21969 | 40% |
反応手順
28 grams of calcium oxide were added to water to form a thick slurry. This slurry was slowly added with stirring to 392 grams of a 50% aqueous solution of technical grade gluconic acid. After all of the slurry was added the resultant mixture was cooled and 61.8 grams of technical grade boric acid added. The mixture was stirred until a dark brown solution was obtained and then adjusted by water addition to provide a 40% solids solution.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04554020 |
| 出典データセット | uspto-grants-1985_11 |
| ORD ID | ord-cf87304846d54a9e9fbd4af92568221d |
| 出典メモ | uspto-grants-1985_11 |