反応式
[CH3:1][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][C:7]=1[CH3:8].S(=O)(=O)(O)O.[CH3:14][CH:15]([NH2:23])[CH2:16][CH2:17][CH2:18][C:19](O)([CH3:21])[CH3:20].Cl>CO>[NH2:23][CH:15]([CH2:16][CH2:17][CH2:18][C:19]([C:4]1[CH:5]=[CH:6][C:7]([CH3:8])=[C:2]([CH3:1])[CH:3]=1)([CH3:21])[CH3:20])[CH3:14]参加物
5
実験手順
21.2 Parts of o-xylene, 128 parts of 98% w/w sulphuric acid, 24 parts of methanol, and 36.3 parts of heptaminol hydrochloride were stirred at room temperature for 3 days. The work up was carried out as described in Example 2 and gave on distillation 36.2 parts of 2-amino-6-(3,4-dimethylphenyl)-6-methylheptane b16 164°-8° with the following percentage composition by weight.
出典と根拠
- ORDレコード
- ord-2842386169e142f2a1a2f095751de616
- 出典データセット
- uspto-grants-1985_11
- 特許番号
- US04554379
関連ノート
読み込み中…