5-(3-nitrophenyl)tetrazole → HCID 178507542、化合物

HRID 1588026ノート

反応式

HRID 1588026 の反応式
[N+:1]([C:4]1[CH:5]=[C:6]([C:10]2[NH:14][N:13]=[N:12][N:11]=2)[CH:7]=[CH:8][CH:9]=1)([O-])=O>C(O)C.[Pd]>[NH2:1][C:4]1[CH:5]=[C:6]([C:10]2[NH:14][N:13]=[N:12][N:11]=2)[CH:7]=[CH:8][CH:9]=1

参加物

4

反応物 1

HCID 2851295-(3-nitrophenyl)tetrazole

生成物 1

HCID 178507542HCID 178507542、化合物

試薬・触媒・溶媒 2

HCID 23938Palladium触媒HCID 702Ethanol溶媒

実験手順

3-Nitro-(1H-tetrazol-5-yl)benzene was dissolved in 200 ml of ethanol, treated with 1.7 g of 10% palladium/carbon catalyst, and hydrogenated on a Parr apparatus at 30 psi for 2 hours. The reaction mixture was filtered through Celite and concentrated to give 4.7 g of the title compound.

後処理

  1. filtrationThe reaction mixture was filtered through Celite
  2. concentrationconcentrated

出典と根拠

ORDレコード
ord-8011f81aac654496807dfbdc36505afe
出典データセット
uspto-grants-1993_06
特許番号
US05220018

反応ノート

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