Glycine → Glyphosate

反応式

[CH:1]([P:3](=[O:6])([OH:5])[OH:4])=O.[NH2:7][CH2:8][C:9]([OH:11])=[O:10]>>[CH2:8]([NH:7][CH2:1][P:3]([OH:4])([OH:5])=[O:6])[C:9]([OH:11])=[O:10]

参加物

反応物 2

HCID 750Glycine

HCID 10154022Formylphosphonic Acid

生成物 1

HCID 3496Glyphosate収率 90%

実験手順

Reaction of formylphosphonic acid and glycine was carried out under the conditions described in Example 6 except that the pH was adjusted to 10.0 before commencement of the reduction reaction. Analysis indicated a 90.0% yield of glyphosate salts.

後処理

customwas adjusted to 10.0 before commencement of the reduction reaction

出典と根拠

ORDレコード: ord-cef81218ec8b444099534f6233389600
出典データセット: uspto-grants-1986_02
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04568432

反応ノート

読み込み中…