Glycine → Glyphosate
反応式
[NH2:1][CH2:2][C:3]([OH:5])=[O:4].[CH:6]([P:8](=[O:11])([OH:10])[OH:9])=O.[H][H]>>[CH2:2]([NH:1][CH2:6][P:8]([OH:11])([OH:10])=[O:9])[C:3]([OH:5])=[O:4]参加物
4
実験手順
Reaction of glycine and formylphosphonic acid was carried out under the conditions of Example 2 except that the pH was initially adjusted to 8.0 and hydrogen gas was continuously bubbled through the liquid phase at atmospheric pressure. After 18 hours of reaction, a 65.9% yield of glyphosate was obtained.
後処理
- customwas continuously bubbled through the liquid phase at atmospheric pressure
- customAfter 18 hours of reaction
出典と根拠
- ORDレコード
- ord-535ff560ff9748c89d09a51ee93b2d3b
- 出典データセット
- uspto-grants-1986_02
- 特許番号
- US04568432
反応ノート
読み込み中…