反応式
[NH2:1][CH2:2][C:3]([OH:5])=[O:4].C(=O)([O-])O.[Na+].[NH:11]([C:32]([O:34][C:35]([CH3:38])([CH3:37])[CH3:36])=[O:33])[C@H:12]([C:22](ON1C(=O)CCC1=O)=[O:23])[CH2:13][O:14][CH2:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>C1COCC1>[NH:11]([C:32]([O:34][C:35]([CH3:38])([CH3:37])[CH3:36])=[O:33])[C@H:12]([C:22]([NH:1][CH2:2][C:3]([OH:5])=[O:4])=[O:23])[CH2:13][O:14][CH2:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1参加物
5
実験手順
To an aqueous solution containing 6.80 g of H-Gly-OH and 9.20 g of sodium hydrogen carbonate, under ice-cooling condition, was added 120 ml of THF solution containing 27.5 g of Boc-Ser(Bzl)-OSu, and the mixture was stirred at room temperature overnight.
後処理
- temperatureunder ice-cooling condition
出典と根拠
- ORDレコード
- ord-f981639275ce4afcb212119f5339d2a8
- 出典データセット
- uspto-grants-1993_04
- 特許番号
- US05204326
関連ノート
読み込み中…