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Formaldehyde → Formaldehyde, polymer with 1,3-benzenediol and phenol

HRID 1594536
ノート
印刷プレビュー

反応式

HRID 1594536 の反応式
[C:1]1([CH:8]=[CH:7][CH:6]=[C:4]([OH:5])[CH:3]=1)[OH:2].[C:9]1([OH:15])[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1.C=O>>[C:1]1([CH:8]=[CH:7][CH:6]=[C:4]([OH:5])[CH:3]=1)[OH:2].[CH2:9]=[O:15].[C:9]1([OH:15])[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1
参加物実験手順後処理出典と根拠反応ノート

参加物

3

反応物 2

HCID 712Formaldehyde2 回HCID 22639633HCID 22639633、化合物

生成物 1

HCID 117702Formaldehyde, polymer with 1,3-benzenediol and phenol

実験手順

A resorcinol-phenol-formaldehyde gluing system was prepared according to conventional technology by stirring 100 parts by weight of a resorcinol-phenol mixture and 20 parts by weight of an aqueous formaldehyde solution containing 40 percent by weight of formaldehyde. After said stirring the glue was applied to a surface in an amount of 400 g/m2. The formaldehyde (HCHO) concentration above said surface was analysed by sucking air through a filter impregnated with dinitrophenylhydrazine, leaching the filter with acetonitrile, and then analysing the extract, by means of HPLC, with regard to the content of HCHO. The volume of analysed air was 28.42 liters, which passed the filter with a flow of 0.98 liters/minute. The results of the analysis are set forth in the Table below.

後処理

  1. concentrationThe formaldehyde (HCHO) concentration above said surface
  • filtrationfilter with acetonitrile
  • filtrationfilter with a flow of 0.98 liters/minute
  • customThe results of the analysis
  • 出典と根拠

    ORDレコード
    ord-6aede6b675634daea5480bf35e4fcae1
    出典データセット
    uspto-grants-2001_09
    DOI
    10.6084/m9.figshare.5104873.v1
    特許番号
    US06284090B1

    反応ノート

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