2-(N-ethyl-m-toluidino)ethanol → 2-(N-Ethyl-m-toluidino)ethyl benzoate

HRID 1599198

反応式

HRID 1599198 の反応式
[C:1](Cl)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:10]([N:12]([CH2:20][CH2:21][OH:22])[C:13]1[CH:18]=[CH:17][CH:16]=[C:15]([CH3:19])[CH:14]=1)[CH3:11]>CC(C)=O.N1C=CC=CC=1>[CH3:19][C:15]1[CH:14]=[C:13]([CH:18]=[CH:17][CH:16]=1)[N:12]([CH2:10][CH3:11])[CH2:20][CH2:21][O:22][C:1](=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

参加物

5

反応物 2

HCID 70672-(N-ethyl-m-toluidino)ethanolHCID 7412Benzoyl chloride

生成物 1

HCID 30162602-(N-Ethyl-m-toluidino)ethyl benzoate

試薬・触媒・溶媒 2

HCID 180Acetone溶媒HCID 1049Pyridine溶媒

実験手順

Benzoylchloride (3.3 g) was added to a mixture of N-ethyl-N-hydroxyethyl-3-methylaniline (2.1 g) in acetone (25 cm3) and pyridine (1 cm3) and stirred at reflux for 1 hour. The reaction mixture was cooled and used directly in iv) below.

後処理

  1. temperatureat reflux for 1 hour
  2. temperatureThe reaction mixture was cooled

出典と根拠

ORDレコード
ord-8bb22e8b3b4743d79c25ce656d2612d5
出典データセット
uspto-grants-1998_04
特許番号
US05739299

関連ノート

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