Hydrochloric Acid → Phenyl octanoate

HRID 1599522ノート

反応式

HRID 1599522 の反応式
[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:8](O)(=[O:16])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15].S(=O)=O.Cl>S(Cl)(Cl)=O>[C:8]([O:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)(=[O:16])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15]

参加物

6

反応物 4

HCID 313Hydrochloric AcidHCID 379Octanoic AcidHCID 996PhenolHCID 1119Sulfur Dioxide

生成物 1

HCID 229895Phenyl octanoate

試薬・触媒・溶媒 1

HCID 24386Thionyl Chloride溶媒

実験手順

The ester was prepared by slowly adding thionyl chloride (10 ml) to a mixture of pure phenol (6.5 g) and octanoic acid (10 g). The reaction mixture was warmed to drive off the sulfur dioxide and hydrogen chloride gases. The crude mixture was distilled at 95°-100° C./5 mmHg.

後処理

  1. temperatureThe reaction mixture was warmed
  2. distillationThe crude mixture was distilled at 95°-100° C./5 mmHg

出典と根拠

ORDレコード
ord-2c67f39815a040c1b539b782c2b2c497
出典データセット
uspto-grants-1998_04
特許番号
US05741821

反応ノート

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