Methyl vinyl ketone → HCID 21829922、化合物
反応式
[CH:1]([C:3]([CH3:5])=[O:4])=[CH2:2].[Cl:6][C:7]1[CH:12]=[CH:11][C:10]([Cl:13])=[CH:9][C:8]=1[NH:14][C:15](=[O:20])[C:16]([NH2:19])([CH3:18])[CH3:17]>O1CCCC1>[Cl:6][C:7]1[CH:12]=[CH:11][C:10]([Cl:13])=[CH:9][C:8]=1[NH:14][C:15](=[O:20])[C:16]([NH:19][CH2:2][CH2:1][C:3](=[O:4])[CH3:5])([CH3:17])[CH3:18]参加物
4
実験手順
Methyl vinyl ketone (1.02 g) was added to a solution of N-(2,5-dichlorophenyl)-2-aminoisobutyramide (2.4 g) in tetrahydrofuran (10 mL) and the mixture was heated at reflux 30 hours. After distilling off the solvent under reduced pressure, 3 g of N-(2,5-dichlorophenyl)-2-(3-oxobutylamino)isobutyramide was obtained.
後処理
- temperaturethe mixture was heated
- temperatureat reflux 30 hours
- distillationAfter distilling off the solvent under reduced pressure
出典と根拠
- ORDレコード
- ord-88f9a1e684d14fed93cc8ab79e568b4b
- 出典データセット
- uspto-grants-1999_11
- 特許番号
- US05977027
反応ノート
読み込み中…