N,N-dimethyl-2-nitrobenzamide → 2-Amino-N,N-dimethylbenzamide
反応式
[CH3:1][N:2]([CH3:14])[C:3](=[O:13])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[N+:10]([O-])=O>[Pd].CO>[CH3:1][N:2]([CH3:14])[C:3](=[O:13])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[NH2:10]参加物
4
実験手順
Palladium on charcoal (0.54 g, 10% Pd by weight) was added to a solution of 2.1 g N,N-dimethyl-2-nitrobenzamide in 150 mL methanol. The resulting suspension was hydrogenated at room temperature at atmospheric pressure for three hours. After filtration of the catalyst, the solvent was removed in vacuo affording N,N-dimethyl-2-aminobenzamide (1.8 g).
後処理
- filtrationAfter filtration of the catalyst
- customthe solvent was removed in vacuo
出典と根拠
- ORDレコード
- ord-22b2c6b43ef84da4aab3379d9e193b3c
- 出典データセット
- uspto-grants-1999_11
- 特許番号
- US05985837
反応ノート
読み込み中…