化工社化工社 化学情報印刷レポート · 研究参考用
Potassium Carbonate → Ethyl 4-(3,4,5-trimethoxyphenoxy)butanoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | Ethyl 4-bromobutyrate | HCID 76300 | — |
| 反応物 | 2,3,4-Trimethoxyphenol | HCID 603577 | — |
| 溶媒 | Methyl Ethyl Ketone | HCID 6569 | — |
| 生成物 | Ethyl 4-(3,4,5-trimethoxyphenoxy)butanoate | HCID 11289513 | — |
反応手順
9.2 g of trimethoxyphenol, 14 g of potassium carbonate and 10.7 g of ethyl 4-bromobutanoate in 150 ml of 2-butanone are refluxed for 24 hours. The mineral salts are then filtered off and the solvent is distilled off under reduced pressure, enabling the expected compound to be obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06992085B2 |
| 出典データセット | uspto-grants-2006_01 |
| ORD ID | ord-029f660a4bf0481fa87428c8836f6e6b |
| 出典メモ | uspto-grants-2006_01 |