HRID1611974

反应详情

EQUATION

反应方程式

HRID 1611974 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

9.2 g of trimethoxyphenol, 14 g of potassium carbonate and 10.7 g of ethyl 4-bromobutanoate in 150 ml of 2-butanone are refluxed for 24 hours. The mineral salts are then filtered off and the solvent is distilled off under reduced pressure, enabling the expected compound to be obtained.

WORKUP

后处理

  1. filtrationThe mineral salts are then filtered off
  2. distillationthe solvent is distilled off under reduced pressure
  3. customto be obtained