Benzyl Alcohol → Benzyl sulfamate
反応式
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[CH2:6]([OH:13])[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1>>[S:1]([O:13][CH2:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)(=[O:4])(=[O:3])[NH2:2]参加物
3
実験手順
The title compound was prepared by the procedures of Example 33 from sulfamoyl chloride and benzyl alcohol being careful to use reduced pressure at about 35° C. to remove solvents in order to avoid violent decomposition observed in another trial at higher temperature. A white solid, mp 75°-78° C., was obtained in 38% yield.
後処理
- customat about 35° C.
- customto remove solvents in order
- customA white solid, mp 75°-78° C., was obtained in 38% yield
出典と根拠
- ORDレコード
- ord-98549ebc5a644c70a0efd1f1ff437bbc
- 出典データセット
- uspto-grants-1993_03
- 特許番号
- US05194446
反応ノート
読み込み中…