1-Methyl-4-piperidone → 1-Methylpiperidin-4-one oxime

HRID 1630421

反応式

HRID 1630421 の反応式
[CH3:1][N:2]1[CH2:7][CH2:6][C:5](=O)[CH2:4][CH2:3]1.Cl.[NH2:10][OH:11]>>[CH3:1][N:2]1[CH2:7][CH2:6][C:5](=[N:10][OH:11])[CH2:4][CH2:3]1

参加物

3

反応物 2

HCID 740491-Methyl-4-piperidoneHCID 443297Hydroxyamine hydrochloride

生成物 1

HCID 3390531-Methylpiperidin-4-one oxime

実験手順

1-Methyl-piperidin-4-one oxime was prepared from 1-methyl-piperidin-4-one and hydroxylamine hydrochloride using conditions of General Method 1. 1H NMR (400 MHz, DMSO-d6) δ 10.31 (1H, s), 2.45 (2H, t, 6.1 Hz), 2.38 (2H, t, 5.9 Hz), 2.31 (2H, t, J=6.0 Hz), 2.20 (2H, t, 6.4 Hz), 2.18 (3H, s).

出典と根拠

ORDレコード
ord-957acd2808654ee7b294fddd7274c4fa
出典データセット
uspto-grants-2014_07
特許番号
US08791134B2

関連ノート

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